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海龟大脑样品 1H 实验

1H experiment on turtle brain sample
1D CPMG filtered 1H experiment on a 20 mg sample of turtle brain with D2O. A vertical expansion of the downfield region shows low level metoblites present in the sample. Data was acquired at 500 MHz using a 4 mm TXI hr-MAS probe with Z-gradient, 64 scans,

老鼠肾脏

TOCSY  on a 21 mg sample of mouse kidney
2D Rotor Synchronized Adiabatic TOCSY with WATERGATE water suppression on a 21 mg sample of mouse kidney Data was acquired at 500 MHz using a 4 mm TXI hr-MAS probe with Z-gradient, 2250 Hz sample spin rate.