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Unbuffered Male Urine Sample

Unbuffered Male Urine Sample

Sample: 350 µl unbuffered male urine in shaped sample tube

Top: Presat ns = 8

Left: HSQC aromatic region

Right: 2D J-RES aliphatic region

Sample: 350 µl unbuffered male urine in shaped sample tube

Top: Presat ns = 8

Left: HSQC aromatic region

Right: 2D J-RES aliphatic region

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Protonless HiRes Bio-NMR

Protonless HiRes Bio-NMR

Protonless HiRes Bio-NMR: 3D CBCACO-IPAP of 1mM Ubiquitin 15N/13C labeled, taken at 600 MHz (ns=2,TD=1024x64x256, experiment time 10 hours)

Protonless HiRes Bio-NMR: 3D CBCACO-IPAP of 1mM Ubiquitin 15N/13C labeled, taken at 600 MHz (ns=2,TD=1024x64x256, experiment time 10 hours)

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2D 13C observe TOCSY

2D 13C observe TOCSY

2D 13C observe TOCSY with 31P & 15N & 1H decoupling, 4 mg 15N/13C labeled RNA 14-mer, experiment time 40 minutes

2D 13C observe TOCSY with 31P & 15N & 1H decoupling, 4 mg 15N/13C labeled RNA 14-mer, experiment time 40 minutes

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1H-15N NN-COSY

1H-15N NN-COSY

1H-15N NN-COSY (H Bond correlation) of 4 mg (~2mM) 15N/13C labeled RNA 14-mer, taken at 600 MHz (ns=8, td= 2kx128, experiment time 25 min, te= 283K).

*RNA standards by Silantes GmbH

1H-15N NN-COSY (H Bond correlation) of 4 mg (~2mM) 15N/13C labeled RNA 14-mer, taken at 600 MHz (ns=8, td= 2kx128, experiment time 25 min, te= 283K).

*RNA standards by Silantes GmbH

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