Energy drinks present complex multicomponent matrices with challenges for routine analysis in food and CPG laboratories. This application note describes an automated qNMR workflow based on 400 MHz NMR and Advanced Chemical Profiling 2.0 for simultaneous identification and quantification of key constituents, including sugars, sweeteners, caffeine, organic acids, and solvents. Minimal sample preparation and automated acquisition, processing, and reporting enable reproducible, high throughput analysis. The approach supports formulation studies, batch release testing, and consistency assessment while providing quantitative results aligned with label claims and regulatory requirements.