TEM PicoIndenter Series

Hysitron PI 95

Quantitative nanomechanical testing inside your transmission electron microscope

Hysitron PI 95 TEM PicoIndenter

Bruker’s Hysitron PI 95 TEM PicoIndenter is the first full-fledged depth-sensing indenter capable of direct-observation nanomechanical testing inside a transmission electron microscope (TEM). With this side-entry instrument, it is not only possible to image the mechanical response of nanoscale materials, but also to acquire load-displacement data simultaneously. Further, an integrated video interface allows for time synchronization between the load-displacement curve and the corresponding TEM video.

Full-fledged
depth-sensing indenter
Enables direct-observation nanomechanical testing inside a transmission electron microscope and supports compression, tension, Push-to-Pull (PTP), Electrical Push-to-Pull (EPTP), nanoDynamic, high temperature, and electrical characterization.
Performech
advanced control module
Delivers a 78 kHz feedback rate and data acquisition up to 38 kHz to capture transient events, such as dislocation bursts.
Precise
tip-positioning and mechanical testing
Includes a three-axis positioner, 3D piezoelectric actuator, and advanced transducer for electrostatic actuation and capacitive displacement sensing.
Features

Customized Solution for Your TEM

The Hysitron PI 95 has been carefully designed for compatibility with JEOL, FEI, Hitachi, and Zeiss microscopes. With this instrument it is not only possible to image the mechanical response of nanoscale materials, but also acquire quantitative mechanical data simultaneously. The integrated video interface allows for synchronization between the load-displacement curve and the corresponding TEM video.

Optimized for Nanoscale Investigation

Dark-field TEM images of a Ni nanopillar before and after compression. The high dislocation density initially observed in the pillar has disappeared upon compression. Nature Materials 7, 115-119 (2007).

The Hysitron PI 95 is uniquely suited for the investigation of nanoscale phenomena. Performing these types of studies in the TEM can provide unambiguous differentiation between the many possible causes of force or displacement transients which may include dislocation bursts, phase transformations, spalling, shear banding or fracture onset.

Unparalleled Performance

An example 1 μN scratch test: (1) Normal and lateral loads and displacements versus time and (2-5) corresponding frames from the in-situ TEM video showing the buckling of the DLC film in advance of the tip and flattening of the asperities in the tops of the grains.

The Hysitron PI 95 utilizes three levels of control for tip positioning and mechanical testing. In addition to a three-axis coarse positioner and a 3D piezoelectric actuator for fine positioning, the instrument is equipped with a transducer for electrostatic actuation and capacitive displacement sensing for acquiring quantitative nanoscale mechanical data.

Upgrade Options and Add-Ons

Expand PI 95 TEM's Capabilities

LEARN MORE:

Contact us for more information about available upgrade options and how PI 95 TEM can be configured to meet your specific measurement needs now and grow with your research going forward.

Webinars

Watch our Recent Broadcasts on Nanomechanics in SEM

Our webinars cover best practices, introduce new products, provide quick solutions to tricky questions, and offer ideas for new applications, modes or techniques.

Hysitron PI 95 TEM FAQ

Frequently Asked Questions

What is a PI 95 TEM PicoIndenter used for?

In-situ mechanical testing inside a TEM to measure nanoscale mechanical, electrical, and functional properties of materials with simultaneous high-resolution imaging.

What types of tests can be performed?

Nanoindentation, compression, tension (with PTP), bending, fatigue, fracture, creep, strain-rate loading, and electromechanical testing (with E-PTP).

What samples can be studied?

1D (nanowires, nanopillars, fibers), 2D (films, membranes, graphene), and 3D microstructures, as well as interfaces (grain boundaries, multilayers, joints).

What makes TEM PicoIndenters unique compared to SEM PicoIndenters?

Direct atomic- to nanoscale observation of deformation, defect nucleation, dislocation motion, fracture, and phase transformations with nanometer resolution.

What is the load/displacement range of PI 95?

Typically, the systems can reach up to 1–2 mN load and 1–2 μm of displacement, sufficient for most nanostructures and thin films.

How do you prepare samples for TEM PicoIndenter testing?

Focused ion beam (FIB) milling or microfabrication methods are commonly used to prepare site-specific TEM lamellae, nanopillars, or suspended structures.

What are the main application areas for a TEM PicoIndenter?

The most common applications include nanomechanics of metals, semiconductors, ceramics, polymers, 2D materials, battery/electrochemical materials, and MEMS/NEMS, as well as thin film reliability and defect dynamics studies.

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