XFlash® FlatQUAD 2L: Annular EDS Detector

Taking Energy Dispersive X-ray Spectroscopy to New Limits

XFlash FlatQUAD 2L is a unique and industry-leading Energy Dispersive X-ray Spectroscopy (EDS) detector with an annular 4-channel design that maximizes signal collection to open up new application areas for EDS.

The latest design of the XFlash FlatQUAD detector includes an enlarged central aperture, to enable simultaneous BSE imaging, all without impacting our industry-leading output count rates of 4,000,000 cps. 

XFlash® FlatQUAD 2L - Making Difficult EDS Easy

  • Perform SEM EDS at ultra-high resolutions down to the nanometer scale.
  • Quantify elemental compositions at high throughput.
  • Overlay X-ray EDS signals with simultaneously acquired BSE images. 
  • Analyze the elements in delicate or charging samples.
  • Accurately map the elemental composition of topographic samples.
  • Perform TEM-like EDS using a SEM.
  • Operate in low vacuum and high vacuum mode.

 

XFlash® FlatQUAD 2 is the detector at the heart of our QUANTAX FlatQUAD system for EDS.

The XFlash® FlatQUAD 2L is a unique 4-channel annular detector that sits between the sample and SEM pole piece to maximize EDS signal collection whilst enabling simultaneous BSE imaging. 

A Unique Detector Design for Industry-Leading Performance

The unique and patented design of the XFlash FlatQUAD 2L detector delivers unparalleled performance for both quantitative and qualitative EDS analysis. 

XFlash® FlatQUAD 2L is uniquely constructed, with four silicon drift detector (SDD) segments, of 100 mm2 total area, arranged annularly around a central aperture. 

The detector is positioned between the SEM pole piece and the sample, with the central aperture allowing the primary electron beam to pass through unobstructed.

This configuration significantly increases the solid angle and consequently the X-ray collection efficiency when compared to conventional EDS detector geometries. Additionally, the aperture also enables the efficient collection of backscattered electrons using the SEM’s BSE detectors, allowing true parallel signal acquisition.

To ensure compatibility with many different SEM types, XFlash® FlatQUAD 2L can be precisely positioned in the X, Y and Z directions.

Schematic showing how the primary electron beam of the SEM passes through the opening in the center of the XFlash® FlatQUAD 2L.

The X-ray signal emitted from the sample (magenta) is collected by the four SDD segments surrounding this opening, maximizing the solid angle and collection efficiency, whilst backscattered electrons (blue) pass back through to the SEM pole piece for BSE imaging.

Efficient EDS Signal Collection with an Output Count Rate of 4,000,000 cps 

XFlash FlatQUAD solid angle and OCR as a function of detector-sample distance plot of the output count rate (OCR) that can be achieved on copper at 5 kV accelerating voltage, 1 nA beam current and the according detector solid angle, theoretically calculated according to Nestor J. Zaluzec, Detector Solid Angle Formulas

The orthogonal positioning of the XFlash® FlatQUAD 2L detector results in the largest solid angle yet for X-ray collection in a SEM.

Solid angles of more than 1 sr and take-off angles of more than 60° are possible with XFlash® FlatQUAD 2L, depending on specific geometrical conditions, to deliver extremely high count rates. 

Each of the four detector chips is equipped with its own signal processing channel. This allows input count rates (ICR) of more than 10,000,000 cps and a combined output count rate (OCR) of up to 4,000,000 cps to be reached for ultra-fast and ultra-sensitive EDS.

XFlash® FlatQUAD 2L has an excellent energy resolution of 127 eV at Mn Kα. Resolution classes of 129 eV and 133 eV are also available.

New feature

True Parallel BSE and EDS Imaging 

The large central aperture of the XFlash® FlatQUAD 2L EDS detector facilitates the unobstructed transmission of backscattered electrons to retractable or in-lens BSE detectors.

As a result, high-resolution BSE imaging can be performed in parallel with EDS acquisition for the simultaneous acquisition of compositional (EDS) and chemical (BSE) information.

Specialized polymer detector windows of variable thickness enable the controlled separation and simultaneous utilization of BSE and X-ray signals, depending on application requirements. These windows are optimized to manage backscattered electron interaction while maintaining a high X-ray transmission efficiency.

Low-kV EDS mapping of NMC811 particles acquired at 3 kV and 3.2 nA. The smaller interaction volume at 3 kV improves surface sensitivity while high collection efficiency of XFlash® FlatQUAD 2L gives an output count rate of 157,000 cps, enabling high-quality elemental maps within a few minutes.
Low-kV EDS mapping of NMC811 particles acquired at 3 kV and 3.2 nA. The smaller interaction volume at 3 kV improves surface sensitivity while high collection efficiency of XFlash® FlatQUAD 2L gives an output count rate of 157,000 cps, enabling high-quality elemental maps within a few minutes.

Applications of XFlash® FlatQUAD 2L

The unique geometry of the XFlash® FlatQUAD 2L detector makes challenging EDS easy, opening up whole new application areas to EDS analysis. 

  • Nanostructured samples – Ultra-high resolution for the analysis of samples with nanoscale features, such as semiconductors and advanced coatings. 
  • Non-conductive samples – Low kV analysis of poorly charging samples including polymers, ceramics and pharmaceutical materials. 
  • Topographic and rough samples – Improved X-ray collection from uneven surfaces including particles, fibers and additively manufactured components.
  • Beam sensitive samples – Elemental mapping of beam sensitive samples, such as biological specimens, at low beam currents. 
  • Electron transparent samples  Using STEM in SEM imaging. 

Learn more about the wide range of EDS applications that are now possible when using XFlash® FlatQUAD 2L on the QUANTAX FlatQUAD page. 

Elemental map of a sea worm sample taken using an XFlash® FlatQUAD detector. 

Discover QUANTAX FlatQUAD

XFlash® FlatQUAD 2L is the detector at the core of our QUANTAX FlatQUAD analytical system. 

QUANTAX FlatQUAD includes everything you need to perform ultra-signal-efficient SEM EDS, including an XFlash® FlatQUAD 2L detector, processing electronics and our comprehensive ESPRIT software suite.